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异型坩埚

异型坩埚

发布时间:2018-07-12点击量:34
异型坩埚

1.坩埚属陶瓷制品,坩埚壁内存在一定数量的气孔,容易吸潮,所以首次使用坩埚之前在不加料的条件下,坩埚必须进行预热以确保没有湿气残留在坩埚壁中:最好是放在有温度的炉边烘烤24小时以上,在这段时间内,坩埚要转动几次,使其均匀受热,去除坩埚壁内的潮气(或者将适量木柴放置坩埚内燃烧3小时左右达到预热效果)。以免坩埚升温太快,造成坩埚热膨胀,出现掉底、脱层或爆裂。

注:潮气一般在75~100度时蒸发的快,所以在此温度时升温一定要慢;2小时后坩埚预热至150~200度并保温一小时,之后每小时升温150度。由于在315~650度的温度范围内坩埚壁会出现快速氧化,氧化不仅会缩短坩埚的寿命,而且会由于热导率降低影响其使用性能,因此坩埚无需在此温度区间内停留过久的时间。

2.坩埚经过第一次预热后通常如连续使用无需再次预热,除非坩埚再次暴露于潮湿的环境中

3.坩埚预热后,操作人员需要在不加料的状态下快速升温到850~950度,并保温半小时,再降到正常的使用温度,然后加料。(加热坩埚使其温度高于正常工作温度会延长坩埚的使用寿命。)通常使坩埚加热至815~930度,会有助于坩埚的釉料保护,如果有可能,这种高温加热可以每周都进行一次


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